1-Phenethylamine → Ethyl 2-(1-phenylethylamino)cyclohexene-1-carboxylate

HRID 813465Notes

Reaction equation

HRID 813465 reaction equation
[F:22][C:23]([F:24])([F:25])[S:26]([O-:27])(=[O:28])=[O:29].[F:31][C:32]([F:33])([F:34])[S:35]([O-:36])(=[O:37])=[O:38].[F:39][C:40]([F:41])([F:42])[S:43]([O-:44])(=[O:45])=[O:46].[O:1]=[C:2]1[CH:3]([C:8](=[O:9])[O:10][CH2:11][CH3:12])[CH2:4][CH2:5][CH2:6][CH2:7]1.[Yb+3:30].[c:13]1([CH:19]([CH3:20])[NH2:21])[cH:14][cH:15][cH:16][cH:17][cH:18]1>>[C:2]1([NH:21][CH:19]([c:13]2[cH:14][cH:15][cH:16][cH:17][cH:18]2)[CH3:20])=[C:3]([C:8](=[O:9])[O:10][CH2:11][CH3:12])[CH2:4][CH2:5][CH2:6][CH2:7]1

Participants

5

Reactant 4

HCID 74081-PhenethylamineHCID 95543Ethyl 2-oxocyclohexanecarboxylateHCID 105055Ytterbium(3+)HCID 2758875Trifluoromethanesulfonate3×

Product 1

HCID 11778072Ethyl 2-(1-phenylethylamino)cyclohexene-1-carboxylate

Sources & evidence

ORD record
ord-f32f1f22db4d43a7b72213fd00e38d64
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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