돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 81502생성일: 2026년 10월 25일

Water → tert-Butyl [2,6-dimethyl-4-(5-methylsulfanyl-7-propoxyoxazolo[5,4-d]pyrimidin-2-yl)-phenoxy]acetate

https://huagongshe.com/reaction/81502

반응식

참여 물질

역할이름HCID투입량
반응물WaterHCID 962—
반응물Potassium CarbonateHCID 11430—
반응물tert-Butyl bromoacetateHCID 79177—
반응물HCID 136389866HCID 136389866—
용매DimethylformamideHCID 6228—
생성물tert-Butyl [2,6-dimethyl-4-(5-methylsulfanyl-7-propoxyoxazolo[5,4-d]pyrimidin-2-yl)-phenoxy]acetateHCID 86688232—

반응 단계

3.20 g of potassium carbonate and then 0.93 ml of tert-butyl bromoacetate were added to a solution of 2.00 g of 2,6-dimethyl-4-(5-methylsulfanyl-7-propoxyoxazolo[5,4-d]pyrimidin-2-yl)phenol in 20 ml of N,N-dimethylformamide. The mixture was reacted at 60° C. for 1 h and then allowed to cool and poured into water. The precipitate obtained was filtered off with suction and dried under reduced pressure. This gave 2.45 g of the title compound.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08846691B2
출처 데이터셋uspto-grants-2014_09
ORD IDord-1fe2590e9b5b43a697d634712d8aefba
출처 메모uspto-grants-2014_09