Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,4,5-Trimethoxyaniline → N-(3-(2-(3,4,5-trimethoxyphenylamino)pyrimidin-4-ylthio)phenyl)acrylamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,4,5-Trimethoxyaniline | HCID 32285 | — |
| 반응물 | N-(3-(2-chloropyrimidin-4-ylthio)phenyl)acrylamide | HCID 86645569 | — |
| 생성물 | N-(3-(2-(3,4,5-trimethoxyphenylamino)pyrimidin-4-ylthio)phenyl)acrylamide | HCID 59491639 | 14% |
반응 단계
In a procedure analogous to Example 8, reaction of N-(3-(2-chloropyrimidin-4-ylthio)phenyl)acrylamide (100 mg, 0.34 mmol) and 3,4,5-trimethoxyaniline (75 mg, 0.41 mmol) furnished the product (20 mg, 14%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08846704B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-c6ab1dea59d649a9957a355da4620c12 |
| 출처 메모 | uspto-grants-2014_09 |