4-Carboxyphenylboronic Acid → 4'-((N-(3-(Benzyloxy)-4-((Benzyloxy)Carbonyl)Phenyl)-2-(N,4-Dimethylphenylsulfonamido)Acetamido)Methyl)-[1,1'-Biphenyl]-4-Carboxylic Acid

Participants

Role	Name	HCID	Charge
Reactant	4-Carboxyphenylboronic Acid	HCID 312183	—
Reactant	Benzyl 2-(benzyloxy)-4-(N-(4-bromobenzyl)-2-(N,4-dimethylphenylsulfonamido)acetamido)benzoate	HCID 66728422	—
Product	4'-((N-(3-(Benzyloxy)-4-((Benzyloxy)Carbonyl)Phenyl)-2-(N,4-Dimethylphenylsulfonamido)Acetamido)Methyl)-[1,1'-Biphenyl]-4-Carboxylic Acid	HCID 68076757	—

Reaction Steps

Aryl halide 9 was coupled to 4-carboxyphenylboronic acid to give 32 on a 0.1 mmol scale via General Procedure H. 32 was not purified at this stage and was deprotected without purification.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08846707B2
Source dataset	uspto-grants-2014_09
ORD ID	ord-2406dbf09e94407a9d3992c22f8f30ab
Source note	uspto-grants-2014_09