Dichloromethane → tert-Butyl 4-(hydrazinecarbonyl)piperidine-1-carboxylate

HRID 819179Notes

Reaction equation

HRID 819179 reaction equation
[C:17]([c:18]1[nH:19][cH:20][cH:21][n:22]1)([c:23]1[nH:24][cH:25][cH:26][n:27]1)=[O:28].[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH2:10][CH:11]([C:14](=[O:15])[OH:16])[CH2:12][CH2:13]1.[Cl:31][CH2:32][Cl:33].[NH2:29][NH2:30]>>[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH2:10][CH:11]([C:14](=[O:16])[NH:29][NH2:30])[CH2:12][CH2:13]1

Participants

5

Reactant 4

HCID 6344DichloromethaneHCID 9321HydrazineHCID 3928711-(tert-Butoxycarbonyl)-4-piperidinecarboxylic acidHCID 5250894Bis-(1H-imidazol-2-YL)-methanone

Product 1

HCID 22713165tert-Butyl 4-(hydrazinecarbonyl)piperidine-1-carboxylate

Sources & evidence

ORD record
ord-8590e39c1257446ba6a2614a9e01cb1d
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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