Ethyl bromoacetate → HCID 70847734, compound
Reaction equation
[F:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:10]=1[NH:9][N:8]=[CH:7]2.Br[CH2:12][C:13]([O:15][CH2:16][CH3:17])=[O:14]>>[F:1][C:2]1[C:10]2[C:6](=[CH:7][N:8]([CH2:12][C:13]([O:15][CH2:16][CH3:17])=[O:14])[N:9]=2)[CH:5]=[CH:4][CH:3]=1Participants
3
Procedure
The title compound was prepared according to the method described for Preparation 93 using 7-fluoro-1H-indazole and ethyl bromoacetate to afford the title compound as an off-white solid in 35% yield, 175 mg.
Workup
- customThe title compound was prepared
Sources & evidence
- ORD record
- ord-1659ef175f554d65b80a99525cc7a759
- Source dataset
- uspto-grants-2014_09
- Patent number
- US08846698B2
Reaction notes
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