Dichloromethane → 2,4,6-Trimethylbenzene-1-sulfonate

HRID 830174Notes

Reaction equation

HRID 830174 reaction equation
[CH3:15][C:16]([CH3:17])([CH3:18])[Si:19]([O:20][CH2:21][c:22]1[cH:23][cH:24][n:25][cH:26][cH:27]1)([CH3:28])[CH3:29].[Cl:30][CH2:31][Cl:32].[NH2:1][O:2][S:3](=[O:4])(=[O:5])[c:6]1[c:7]([CH3:14])[cH:8][c:9]([CH3:13])[cH:10][c:11]1[CH3:12]>>[NH2:1][n+:25]1[cH:24][cH:23][c:22]([CH2:21][O:20][Si:19]([C:16]([CH3:15])([CH3:17])[CH3:18])([CH3:28])[CH3:29])[cH:27][cH:26]1.[O:2]=[S:3](=[O:4])([O-:5])[c:6]1[c:7]([CH3:14])[cH:8][c:9]([CH3:13])[cH:10][c:11]1[CH3:12]

Participants

5

Reactant 3

HCID 6344DichloromethaneHCID 109878804-(Tert-butyldimethylsilyloxymethyl)pyridineHCID 11830845O-(2,4,6-Trimethylbenzenesulfonyl)hydroxylamine

Product 2

HCID 38762462,4,6-Trimethylbenzene-1-sulfonateHCID 595138064-[[Tert-butyl(dimethyl)silyl]oxymethyl]pyridin-1-ium-1-amine

Sources & evidence

ORD record
ord-9f1c3023139b424ebb698176697b7d70
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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