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HRID8325

反应详情

EQUATION

反应方程式

HRID 8325 的结构方程式

REACTANTS

反应物

2
结构：Cc1nn(C)c(Cl)c1S(=O)(=O)Cl
HCID2777126

5-chloro-1,3-dimethyl-1H-pyrazole-4-sulfonyl chloride

C5H6Cl2N2O2S

结构：CC(C)(C)OC(=O)N1CCN(c2cccc3[nH]ccc23)CC1
HCID22015386

tert-Butyl 4-(1H-indol-4-yl)piperazine-1-carboxylate

C17H23N3O2

PRODUCTS

生成物

1
结构：Cc1nn(C)c(Cl)c1S(=O)(=O)n1ccc2c(N3CCNCC3)cccc21.Cl
HCID10113503

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(4-boc-piperazinyl)-indole and 5-chloro-1,3-dimethyl-1H-pyrazol-4yl-sulfonyl chloride according to Method 3: 1H NMR (270 MHz, DMSO-d6) δ 9.17 (br, 1 H), 7.78 (d, J=3 Hz, 1 H), 7.49 (d, J=8 Hz, 1 H), 7.28 (t, J=8 Hz, 1 H), 6.93 (d, J=3 Hz, 1 H), 6.87 (d, J=8 Hz, 1 H), 3.72 (s, 3 H), 3.28 (m, 8 H), 2.34 (s, 3 H); MS (ESI+) for m/z 394 (M+H)+.