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HRID8326

反应详情

EQUATION

反应方程式

HRID 8326 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)c1cccnc1
HCID3164136

Pyridine-3-sulfonyl chloride

C5H4ClNO2S

结构：CC(C)(C)OC(=O)N1CCN(c2cccc3[nH]ccc23)CC1
HCID22015386

tert-Butyl 4-(1H-indol-4-yl)piperazine-1-carboxylate

C17H23N3O2

PRODUCTS

生成物

1
结构：Cl.O=S(=O)(c1cccnc1)n1ccc2c(N3CCNCC3)cccc21
HCID22015331

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(4-boc-piperazinyl)-indole and 3-pyridinylsulfonyl chloride according to Method 3: 1H NMR (270 MHz, DMSO-d6) δ 9.37 (br, 1 H), 9.18 (d, J=3 Hz, 1 H), 8.86 (d, J=5 Hz, 1 H), 8.39 (d, J=8 Hz, 1 H), 7.85 (d, J=3 Hz, 1 H), 7.70–7.60 (m, 2 H), 7.27 (t, J=8 Hz, 1 H), 7.00 (d, J=3 Hz, 1 H), 6.82 (d, J=8 Hz, 1 H), 3.24 (m, 8 H); MS (ESI+) for m/z 343 (M+H)+.