Diethyl Ether → 1-tert-Butyl 4-ethyl 5-oxoazepane-1,4-dicarboxylate

HRID 833959Notes

Reaction equation

HRID 833959 reaction equation
[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH2:10][C:11](=[O:14])[CH2:12][CH2:13]1.[CH3:23][CH2:24][O:25][CH2:26][CH3:27].[N+:15](=[N-:16])=[CH:17][C:18](=[O:19])[O:20][CH2:21][CH3:22]>>[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH2:10][C:11](=[O:14])[CH:17]([C:18](=[O:19])[O:20][CH2:21][CH3:22])[CH2:12][CH2:13]1

Participants

4

Reactant 3

HCID 3283Diethyl EtherHCID 12192Ethyl diazoacetateHCID 735900tert-Butyl 4-oxopiperidine-1-carboxylate

Product 1

HCID 44365701-tert-Butyl 4-ethyl 5-oxoazepane-1,4-dicarboxylate

Sources & evidence

ORD record
ord-1241b5c9d834469e87bf590fc79b3f11
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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