HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → 4-methoxy-N7-(2-methoxy-ethyl)-N7-methyl-benzothiazole-2,7-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | Acetic Acid Mixture with Hydrobromic Acid | HCID 21893785 | — |
| Reactant | {2-Methoxy-5-[(2-methoxy-ethyl)-methyl-amino]-phenyl}-thiourea | HCID 22015743 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 4-methoxy-N7-(2-methoxy-ethyl)-N7-methyl-benzothiazole-2,7-diamine | HCID 22015744 | — |
Reaction Steps
From {2-methoxy-5-[(2-methoxy-ethyl)-methyl-amino]-phenyl}-thiourea with HBr—AcOH (2 equiv.) and DMSO (1.1 equiv.) in AcOH. ES-MS m/e (%): 268 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07087761B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-225d37cb45ef48c3874c2173b78719eb |
| Source note | uspto-grants-2006_08 |