Potassium Cation → tert-Butyl 4-(5-nitropyridin-2-yl)piperazine-1-carboxylate

HRID 836617Notes

Reaction equation

HRID 836617 reaction equation
[C:17]([CH3:18])([CH3:19])([CH3:20])[O:21][C:22](=[O:23])[N:24]1[CH2:25][CH2:26][NH:27][CH2:28][CH2:29]1.[C:1](=[O:2])([O-:3])[O-:4].[Cl:7][c:8]1[n:9][cH:10][c:11]([N+:14](=[O:15])[O-:16])[cH:12][cH:13]1.[K+:5].[K+:6].[O:30]1[CH2:31][CH2:32][O:33][CH2:34][CH2:35]1>>[c:8]1([N:27]2[CH2:26][CH2:25][N:24]([C:22]([O:21][C:17]([CH3:18])([CH3:19])[CH3:20])=[O:23])[CH2:29][CH2:28]2)[n:9][cH:10][c:11]([N+:14](=[O:15])[O-:16])[cH:12][cH:13]1

Participants

6

Reactant 5

HCID 813Potassium Cation2×HCID 19660Carbonate IonHCID 312751,4-DioxaneHCID 783082-Chloro-5-nitropyridineHCID 143452tert-Butyl piperazine-1-carboxylate

Product 1

HCID 16217943tert-Butyl 4-(5-nitropyridin-2-yl)piperazine-1-carboxylate

Sources & evidence

ORD record
ord-222df96871324da18c579c5038bda50d
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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