HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Butanediol → 1,3-Butadiene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Butanediol | HCID 8064 | — |
| Reactant | 1,4-Diacetoxybutene | HCID 537670 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1,3-Butadiene | HCID 7845 | — |
| Product | Butylene glycol diacetate | HCID 69410 | — |
Reaction Steps
The process for preparing tetrahydrofuran according to claim 1, wherein 1,4-butanediol is prepared by hydrogenating 1,4-diacetoxybutene, which is produced by the acetoxylation of butadiene, into 1,4-diacetoxybutane and hydrolyzing said 1,4-diacetoxybutane as the hydrogenated products in the presence of a solid acid catalyst and distilling hydrolyzates thus obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04093633 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-357e585483c74cd09deece7735851e7f |
| Source note | uspto-grants-1978_06 |