p-Toluenesulfonyl isocyanate → HCID 20325610, compound

HRID 839025Notes

Reaction equation

HRID 839025 reaction equation
[CH2:1]([CH:3]1[CH2:8][C:7](=[O:9])[CH2:6][C:5](=[O:10])[CH2:4]1)[CH3:2].[C:11]1([CH3:23])[CH:16]=[CH:15][C:14]([S:17]([N:20]=[C:21]=[O:22])(=[O:19])=[O:18])=[CH:13][CH:12]=1>C1C=CC=CC=1>[CH2:1]([CH:3]1[CH2:8][C:7](=[O:9])[CH:6]([C:21](=[O:22])[NH:20][S:17]([C:14]2[CH:15]=[CH:16][C:11]([CH3:23])=[CH:12][CH:13]=2)(=[O:18])=[O:19])[C:5](=[O:10])[CH2:4]1)[CH3:2]

Participants

4

Reactant 2

HCID 77703p-Toluenesulfonyl isocyanateHCID 2734798HCID 2734798, compound

Product 1

HCID 20325610HCID 20325610, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

Reaction of 5-ethyl-1,3-cyclohexanedione with p-toluenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 5-ETHYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE, m.p. 86°-87° C. (corr.).

Sources & evidence

ORD record
ord-ac3c6d4c86214beda3bf26d958b64f73
Source dataset
uspto-grants-1978_06
Patent number
US04093741

Reaction notes

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