HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonyl isocyanate → HCID 20325616, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonyl isocyanate | HCID 77703 | — |
| Reactant | 5-Isobutylcyclohexane-1,3-dione | HCID 2736673 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20325616 | HCID 20325616 | — |
Reaction Steps
Reaction of equimolar amounts of 5-isobutyl-1,3-cyclohexanedione with p-toluenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 5-ISOBUTYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE, m.p. 128°-130° C. (corr.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04093741 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-c5df1c769dc045b0890d15c2f161e7f8 |
| Source note | uspto-grants-1978_06 |