HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Acifluorfen sodium
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Acifluorfen | HCID 44073 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Acifluorfen sodium | HCID 44072 | 105.4% |
Reaction Steps
5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (1.7 g, 0.0047 mole) is dissolved in methanol (25 ml) and sodium hydroxide (4.7 ml of 1 N NaOH in methanol, 0.0047 mole) is added rapidly. The solvent is then removed in vacuo to give 1.9 g of product that decomposes at 217° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04093446 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-71444229c592446ba04f2673d332b17b |
| Source note | uspto-grants-1978_06 |