Methylhydrazine → Pyridine, 2-(1-methylhydrazinyl)-

HRID 839213Notes

Reaction equation

HRID 839213 reaction equation

Cl[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][N:3]=1.[CH3:8][NH:9][NH2:10]>COCCO>[CH3:8][N:9]([C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][N:3]=1)[NH2:10]

Participants

4

Reactant 2

HCID 6061Methylhydrazine

HCID 79772-Chloropyridine

Product 1

HCID 77911Pyridine, 2-(1-methylhydrazinyl)-

Reagents, catalysts & solvents 1

HCID 80192-MethoxyethanolSolvent

Procedure

is obtained by boiling an admixture of 2-chloropyridine and methylhydrazine in 2-methoxyethanol under reflux.

Workup

customis obtained
temperatureunder reflux

Sources & evidence

ORD record: ord-302830ca72f74c568868a0cccd20ca0f
Source dataset: uspto-grants-1978_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04093812

Reaction notes

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