Phenol → HCID 20324043, compound

HRID 839259Notes

Reaction equation

HRID 839259 reaction equation
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH:8](=[O:12])/[CH:9]=[CH:10]/[CH3:11]>>[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH:8](=[O:12])/[CH:9]=[CH:10]/[CH3:11]

Participants

3

Reactant 2

HCID 996PhenolHCID 447466Crotonaldehyde

Product 1

HCID 20324043HCID 20324043, compound

Procedure

The phenol silicoformate compound and crotonaldehyde are mixed in about an equal molar ratio then heated to 70° to 90° C while agitating for 20 to 70 minutes, thereby producing a yellow, resinous product, crotonaldehyde phenol silicoformate. The resin is soluble in acetic acid.

Workup

  1. temperaturethen heated to 70° to 90° C

Sources & evidence

ORD record
ord-d52c67dc26644093905b5f1f677baf7a
Source dataset
uspto-grants-1978_06
Patent number
US04094825

Reaction notes

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