Triethylamine → HCID 20324081, compound

Participants

Reaction Conditions

Reaction Steps

20.4 Parts of triethylamine are added to a stirred mixture of 30.4 parts of phenyl N-hydroxycarbamate, 100 parts of dioxan and 38.1 parts of toluenesulphonylchloride at 0° C, keeping the pH in the range 2 to 5. The mixture is then stirred for 18 hours at 25° C and added to 500 parts of water. The oily precipitate is taken up in 500 parts of toluene and the solution is washed with water, dried, filtered and evaporated to constant weight at 40° C under reduced pressure to give 59 parts of phenyl N-p-toluenesulphonyloxycarbamate as a yellow oil.

Provenance & Evidence