HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → HCID 53899637, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Reactant | HCID 54484718 | HCID 54484718 | — |
| Product | HCID 53899637 | HCID 53899637 | 66.7% |
Reaction Steps
In accordance with the process of Preparation 3, potassium t-butoxide (246 mg; 2.2 mmol), thiophenol (220 mg; 2 mmol) and 2-oxo-4-trimethylsilyloxy-bicyclo[3.1.0] hexane-1-carboxylic acid methyl ester (484 mg; 2 mmol) were used to obtain 470 mg of 2-oxo-5-phenylthiomethyl-4-trimethylsilyloxy-cyclopentanecarboxylic acid methyl ester as a viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04094886 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-1b14767ccc134d259128eb8dfb971707 |
| Source note | uspto-grants-1978_06 |