HCID 12862419, compound → HCID 12862420, compound

HRID 839396Notes

Reaction equation

HRID 839396 reaction equation
Cl[CH:2]([C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([O:14][CH3:15])[CH:9]=1)[CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[CH2:16]([Mg]Br)[CH3:17]>[Co](Cl)Cl>[CH3:15][O:14][C:10]1[CH:9]=[C:8]([CH:2]([CH:2]([C:17]2[CH:16]=[CH:8][CH:9]=[C:10]([O:14][CH3:15])[CH:11]=2)[CH2:3][CH2:4][CH2:5][CH2:6][CH3:7])[CH2:3][CH2:4][CH2:5][CH2:6][CH3:7])[CH:13]=[CH:12][CH:11]=1

Participants

4

Reactant 2

HCID 12862419HCID 12862419, compoundHCID 178418443HCID 178418443, compound

Product 1

HCID 12862420HCID 12862420, compound

Reagents, catalysts & solvents 1

HCID 24288Cobalt(II) chlorideCatalyst

Procedure

The preparation was effected in analogy to example 1(c) from 1-chlor-1-(3'-methoxyphenyl)-hexane and ethyl magnesium bromide activated with cobalt - (II) - chloride.

Sources & evidence

ORD record
ord-17109714725048dda4a7c796dee3d8d2
Source dataset
uspto-grants-1978_06
Patent number
US04094994

Reaction notes

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