反应详情

温度

65 °C

To a dry 100 mL round bottom flask equipped with a magnetic stir bar was charged 1.0153 g (8.98×10−3 mol) α-methylene-γ-valerolactone, 16.78 g (0.215 mol) benzene, 0.0561 g (4.31×10−4 mol) divinyl benzene, and 0.0067 g (4.08×10−5 mol) azobisisobutylnitrile. The reactor was purged with nitrogen for 30 minutes before heating to 65° C. The reactor was held at 65° C. for 5 hours before letting cooling the reaction mixture to room temperature and drying under vacuum.

1. customTo a dry 100 mL round bottom flask equipped with a magnetic stir bar
2. customThe reactor was purged with nitrogen for 30 minutes
3. temperaturebefore letting cooling the reaction mixture to room temperature
4. customdrying under vacuum