HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexamethylphosphoramide → Carbamic acid, (7-(phenylthio)imidazo(1,2-a)pyridin-2-yl)-,methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexamethylphosphoramide | HCID 12679 | — |
| Reactant | HCID 13015361 | HCID 13015361 | — |
| Reactant | HCID 21202686 | HCID 21202686 | — |
| Product | Carbamic acid, (7-(phenylthio)imidazo(1,2-a)pyridin-2-yl)-,methyl ester | HCID 329368 | — |
Reaction Steps
A mixture of 2-amino 4-phenylthio pyridine, 1.0 g. (0.00494 mole) and 0.82 g. of methylchloroacetyl carbamate are heated in hexamethylphosphoramide following the procedures of Example 5 to yield 2(methoxycarbonylamino) 7-(phenylthio) imidazo [1,2-a] pyridine, m.p. 221°-223° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04096264 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-967e1e1f09d74cd2aba82a1ce7fc166b |
| Source note | uspto-grants-1978_06 |