5-(Ethanesulfonyl)-2-methoxybenzoic acid → HCID 20190709, compound
Reaction equation
[CH2:1]([S:3]([C:6]1[CH:7]=[C:8]([C:12]([O:15][CH3:16])=[CH:13][CH:14]=1)[C:9](O)=[O:10])(=[O:5])=[O:4])[CH3:2].ClC1C=C(Cl)C=CC=1C[NH:26]CCNCC>>[CH2:1]([S:3]([C:6]1[CH:7]=[C:8]([C:12]([O:15][CH3:16])=[CH:13][CH:14]=1)[C:9]([NH2:26])=[O:10])(=[O:5])=[O:4])[CH3:2]Participants
3
Procedure
By following general method B using 0.9 g. of 3-ethylsulfonyl-6-methoxybenzoic acid and 0.9 g. of N-(2',4'-dichlorophenylmethyl)-N'-ethylethylenediamine, 1.5 g. of N-[2-(N'-2',4'-dichlorophenylmethyl)-N'-ethylamino)ethyl]-3-ethylsulfonyl-6-methoxybenzamide was obtained.
Sources & evidence
- ORD record
- ord-1cf3acfcf41a427a8212a7edd515b906
- Source dataset
- uspto-grants-1978_06
- Patent number
- US04097487
Reaction notes
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