HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 20431454, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-[2-(3-Oxobutyl)phenyl]butanenitrile | HCID 20305108 | — |
| Product | HCID 20431454 | HCID 20431454 | — |
Reaction Steps
A solution of 50 g (0.23 mol) of 4-[2-(3-cyanoproply)phenyl]-2-butanone, 8 in 125 ml glacial acetic acid and 125 ml concentrated HCl was refluxed overnight. The solution was evaporated and the residue diluted with H2O. The precipitate was recrystallized from benzene-petroleum ether to give 42.5 g of the keto acid 9, mp 59°-61° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04097516 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-6d5e2a4138ae4c6399bd61fa9fa27e37 |
| Source note | uspto-grants-1978_06 |