HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 2-Octylcycloprop-2-ene-1-carbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 12474700 | HCID 12474700 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-Octylcycloprop-2-ene-1-carbonyl chloride | HCID 22621645 | 85.4% |
Reaction Steps
A solution of 2-octylcycloprop-2-ene-1-carboxylic acid (350 mg, 1.8 mmol) in ether was treated with 0.45 g (3.5 mmol) of oxalyl chloride at room temperature. The reaction mixture was stirred for one hour then stripped to give 330 mg of 2-octylcycloprop-2-ene-1-carbonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06365549B2 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-3e917755f873453e9da0451521c08301 |
| Source note | uspto-grants-2002_04 |