HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Z)-Benzaldehyde oxime → Methyl 3-phenyl-4-isoxazolecarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Z)-Benzaldehyde oxime | HCID 12143 | — |
| Reactant | HCID 870083 | HCID 870083 | — |
| Product | Methyl 3-phenyl-4-isoxazolecarboxylate | HCID 10750662 | 35% |
Reaction Steps
This compound was synthesised following the procedure described for Compound 8C but using benzaldoxime instead of 4-fluorobenzaldoxime as a starting material. The crude was purified twice by flash chromatography (toluene-acetone 96:4 followed by toluene) to give the title compound as an oil (35%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06365591B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-cfdb9f3188974a09821b1fe5d45b71e2 |
| Source note | uspto-grants-2002_04 |