HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrophenylethyl alcohol → 2-(3-nitrophenyl)acetaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrophenylethyl alcohol | HCID 104058 | — |
| Reactant | 2-Iodoxybenzoic acid | HCID 108794 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-(3-nitrophenyl)acetaldehyde | HCID 11528408 | — |
Reaction Steps
90 mmol of iodoxybenzoic acid are added to 60 mmol of 2-(3-nitrophenyl)ethanol in 300 ml of tetrahydrofuran. The reaction mixture is heated at reflux for 4 hours, then cooled and filtered. The filtrate is concentrated to yield the expected compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06365605B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-29996943fc1d4a4c8cf8dce056347f41 |
| Source note | uspto-grants-2002_04 |