反应详情

120 mmol of thionyl chloride are added to 600 mmol of 4-acetylbenzoic acid in 150 ml of toluene. The reaction mixture is heated at reflux for 3 hours and then cooled. The solvent is evaporated off. The product is used without any other treatment.

1. temperatureThe reaction mixture is heated
2. temperatureat reflux for 3 hours
3. temperaturecooled
4. customThe solvent is evaporated off