化工社化工社 化学情報印刷レポート · 研究参考用
Acetic Acid → HCID 178522205、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | bromine AcOH | HCID 87433071 | — |
| 反応物 | HCID 178522206 | HCID 178522206 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178522205 | HCID 178522205 | 67% |
反応手順
To a solution of the title compound from Example 263 (0.34 grams) and glacial acetic acid (10 mL) was added a 0.7 M bromine-acetic acid solution (4 mL) at 25° C. under N2. After 10 minutes, water was added and the resulting solid was filtered and washed with water several times and dried to give the title compound (Yield 0.31 grams, 67%, MH+ 527).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06365588B1 |
| 出典データセット | uspto-grants-2002_04 |
| ORD ID | ord-a19d0a9bd4154b5086ef088d2f84dff0 |
| 出典メモ | uspto-grants-2002_04 |