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HRID840441

反应详情

EQUATION

反应方程式

HRID 840441 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)CCC(C)(C)c2cc(C(=O)Cl)ccc21
HCID2795466

5,5,8,8-Tetramethyl-5,6,7,8-tetrahydronaphthalene-2-carbonyl chloride

C15H19ClO

结构：COC(=O)c1ccc(C#C[Si](C)(C)C)cc1O
HCID22641103

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1ccc(C#CC(=O)c2ccc3c(c2)C(C)(C)CCC3(C)C)cc1O
HCID15285826

未命名化合物

PROCEDURE

实验过程

Following the basic procedure of Example 1(b), by reacting 2.4 g (0.01 mol) of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthoyl chloride with 2.5 g (0.01 mol) of methyl 2-hydroxy-4-trimethylsilylethynylbenzoate, 2.9 g (74%) of the expected ester, with a melting point of 189°-190° C., were recovered.

WORKUP

后处理

  1. customwith a melting point of 189°-190° C., were recovered