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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 840444Generated: November 1, 2026

Trimethylsilylacetylene → HCID 22619436, compound

https://huagongshe.com/reaction/840444

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrimethylsilylacetyleneHCID 66111—
Reactant6-Bromo-1,1,4,4-tetramethyl-1,2,3,4-tetrahydronaphthaleneHCID 226685—
ProductHCID 22619436HCID 2261943666.1%

Reaction Steps

Following the basic procedure of Example 1(a), by reacting 26.7 g (0.1 mol) of 2-bromo-5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene with 20 g (0.204 mol) of trimethylsilylacetylene, 18.8 g (66%) of the expected compound were obtained in the form of a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06368608B1
Source datasetuspto-grants-2002_04
ORD IDord-a80ba8d4824f495aaedc1fedce473d60
Source noteuspto-grants-2002_04