HuagongsheHuagongshe Chemistry Print Report · For research reference only
8-Benzylidene-1,4-dioxaspiro[4.5]decane → 8-Benzyl-1,4-dioxaspiro[4.5]decane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 8-Benzylidene-1,4-dioxaspiro[4.5]decane | HCID 15417737 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 8-Benzyl-1,4-dioxaspiro[4.5]decane | HCID 10728293 | 99.1% |
Reaction Steps
A solution of 28 g of 8-benzylidene-1,4-dioxa-spiro[4.5]decane and 1 g of 5% palladium on carbon in 250 mL of ethanol was allowed to stir overnight under 1 atm of hydrogen. The catalyst was filtered off and the solution concentrated to give 28 g of 8-benzyl-1,4-dioxa-spiro[4.5]decane as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369076B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-b5c5271a6951410eaf5671d1030a54fd |
| Source note | uspto-grants-2002_04 |