Methyl 2-hydroxy-3-phenylpropanoate → HCID 22462618, compound

HRID 840629Notes

Reaction equation

HRID 840629 reaction equation
[CH2:1]([C:5]1[S:9][C:8]2[CH:10]=[CH:11][CH:12]=[CH:13][C:7]=2[C:6]=1[C:14]1[CH:19]=[CH:18][C:17]([C:20]2[CH:25]=[CH:24][C:23]([OH:26])=[CH:22][CH:21]=2)=[CH:16][CH:15]=1)[CH2:2][CH2:3][CH3:4].C[O:28][C:29](=[O:39])[CH:30]([CH2:32][C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1)O>>[CH2:1]([C:5]1[S:9][C:8]2[CH:10]=[CH:11][CH:12]=[CH:13][C:7]=2[C:6]=1[C:14]1[CH:19]=[CH:18][C:17]([C:20]2[CH:25]=[CH:24][C:23]([O:26][CH:30]([CH2:32][C:33]3[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=3)[C:29]([OH:39])=[O:28])=[CH:22][CH:21]=2)=[CH:16][CH:15]=1)[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 518800Methyl 2-hydroxy-3-phenylpropanoateHCID 10546338HCID 10546338, compound

Product 1

HCID 22462618HCID 22462618, compound

Procedure

The title compound was prepared from 4′-(2-butyl-benzo[b]-thiophen-3-yl)-biphenyl-4-ol, and 3-phenyllactic acid methyl ester, in substantially the same manner, as described in Example 1, steps g-h, and was obtained as a white solid, mp.159-161° C.; MS m/e 507 (M+H)+;

Workup

  1. customwas obtained as a white solid, mp.159-161° C.

Sources & evidence

ORD record
ord-5b0c63cd449845d8951bcc1de936fb0e
Source dataset
uspto-grants-2002_04
Patent number
US06369072B2

Reaction notes

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