Methyl 2-hydroxy-3-phenylpropanoate → HCID 22462572, compound

HRID 840631Notes

Reaction equation

HRID 840631 reaction equation
[C:1]([C:9]1[O:10][C:11]2[CH:30]=[CH:29][CH:28]=[CH:27][C:12]=2[C:13]=1[C:14]1[CH:19]=[CH:18][C:17]([C:20]2[CH:25]=[CH:24][C:23]([OH:26])=[CH:22][CH:21]=2)=[CH:16][CH:15]=1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C[O:32][C:33](=[O:43])[CH:34]([CH2:36][C:37]1[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=1)O>>[C:1]([C:9]1[O:10][C:11]2[CH:30]=[CH:29][CH:28]=[CH:27][C:12]=2[C:13]=1[C:14]1[CH:19]=[CH:18][C:17]([C:20]2[CH:21]=[CH:22][C:23]([O:26][CH:34]([CH2:36][C:37]3[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=3)[C:33]([OH:43])=[O:32])=[CH:24][CH:25]=2)=[CH:16][CH:15]=1)(=[O:8])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 518800Methyl 2-hydroxy-3-phenylpropanoateHCID 10500598HCID 10500598, compound

Product 1

HCID 22462572HCID 22462572, compound

Procedure

The title compound was prepared from 4′-(2-benzoyl-benzofuran-3-yl)-biphenyl-4-ol, and 3-phenyllactic acid methyl ester, in substantially the same manner, as described in Example 1, steps g-h, and was obtained as a yellow solid, mp 159-161° C.; MS m/e 538 (M+);

Workup

  1. customwas obtained as a yellow solid, mp 159-161° C.

Sources & evidence

ORD record
ord-afc7a944ca8b438da7be02eeb9835b24
Source dataset
uspto-grants-2002_04
Patent number
US06369072B2

Reaction notes

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