HRID840641

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID103589

Ethyl 2-hydroxyhexanoate

C8H16O3

结构：Oc1c(Br)cc(-c2ccc(-c3c(Cc4ccccc4)oc4ccccc34)cc2)cc1Br

HCID10506471

未命名化合物

PRODUCTS

生成物

结构：CCCCC(Oc1c(Br)cc(-c2ccc(-c3c(Cc4ccccc4)oc4ccccc34)cc2)cc1Br)C(=O)O

HCID9895791

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4′-(2-benzyl-benzofuran-3-yl)-3,5-dibromo-biphenyl-4-ol, and ethyl DL-2-hydroxycaproate, in substantially the same manner, as described in Example 1, steps g-h , and was obtained as a white solid, mp 75-76° C.; MS m/e 645 (M−H)+;

WORKUP

后处理

customwas obtained as a white solid, mp 75-76° C.

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-b72a65f6b7104227aeeac7163a689bc7
来源数据集: uspto-grants-2002_04
DOI: 10.6084/m9.figshare.5104873.v1
专利: US06369072B2
来源说明: uspto-grants-2002_04

反应 SMILES

[CH2:1]([C:8]1[O:9][C:10]2[CH:31]=[CH:30][CH:29]=[CH:28][C:11]=2[C:12]=1[C:13]1[CH:18]=[CH:17][C:16]([C:19]2[CH:24]=[C:23]([Br:25])[C:22]([OH:26])=[C:21]([Br:27])[CH:20]=2)=[CH:15][CH:14]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:32][CH2:33][CH2:34][CH2:35][CH:36](O)[C:37]([O:39]CC)=[O:38]>>[CH2:1]([C:8]1[O:9][C:10]2[CH:31]=[CH:30][CH:29]=[CH:28][C:11]=2[C:12]=1[C:13]1[CH:18]=[CH:17][C:16]([C:19]2[CH:20]=[C:21]([Br:27])[C:22]([O:26][CH:36]([CH2:35][CH2:34][CH2:33][CH3:32])[C:37]([OH:39])=[O:38])=[C:23]([Br:25])[CH:24]=2)=[CH:15][CH:14]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1