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HRID840732

反应详情

EQUATION

反应方程式

HRID 840732 的结构方程式

REACTANTS

反应物

2
反应SMILES：CC(=O)CC(C)=O
HCID31261

2,4-Pentanedione

C5H8O2

反应SMILES：COc1nn(-c2ccc(N)c(C)c2)c(=O)o1
HCID9877857

未命名化合物

PRODUCTS

产物

1
反应SMILES：COc1nn(-c2ccc(NC(C)=CC(C)=O)c(C)c2)c(=O)o1
HCID69969741

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

The latter compound was obtained by reacting 5-methoxy-3-(4-amino-3-methylphenyl)-3H-(1,3,4)oxadiazol-2-one with equimolar amounts of acetylacetone in glacial acetic acid at 80° C. and was isolated by precipitation by adding water and filtration.

WORKUP

后处理

  1. customThe latter compound was obtained
  2. customat 80° C.
  3. customwas isolated by precipitation
  4. additionby adding
  5. filtrationwater and filtration