Triethylamine → HCID 178472630, compound

Participants

Reaction Steps

A mixture of the compound of Example 10 (0.43 mmol), N-(benzyloxycarbonyloxy)succinimide (107 mg, 0.43 mmol) and triethylamine (0.24 mL, 1.72 mmol) in DMF (3 mL) was stirred at room temperature overnight. The mixture was diluted with ethyl acetate and the organic layer was washed with water three times, dried over anhydrous Na2SO4, filtered and evaporated to give the title compound (195 mg).

Provenance & Evidence