HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 178501524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178427488 | HCID 178427488 | — |
| Product | HCID 178501524 | HCID 178501524 | 100% |
Reaction Steps
A solution of the compound of Example 15 (198 mg) in MeOH at 0° C., was treated with excess thionyl chloride (20 eq). The mixture was stirred at room temperature overnight and evaporated to give the title compound (100% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369063B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-baf42c2a35c04f059aeb15383522106d |
| Source note | uspto-grants-2002_04 |