HuagongsheHuagongshe Chemistry Print Report · For research reference only
8-[Ethoxymethylidene]-6H-[1,3]thiazolo[5,4-e]indol-7-one → HCID 178513208, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 8-[Ethoxymethylidene]-6H-[1,3]thiazolo[5,4-e]indol-7-one | HCID 53990807 | — |
| Reactant | HCID 178513207 | HCID 178513207 | — |
| Product | HCID 178513208 | HCID 178513208 | 26% |
Reaction Steps
The title compound was prepared in 26% yield from 8-ethoxymethylene-6,8-dihydro-1-thia-3,6-diaza-as-indacen-7-one and 4-amino-N-(amino-imino-methyl)-benzenesulfonamide according to Procedure J: 1H NMR (DMSO-d6): δ11.2 (d, 1H), 10.9 (s, 1H), 9.3 (s, 1H), 8.1 (d, 1H), 7.85 (d, 1H), 7.8 (d, 2H), 7.5 (d, 2H), 7.4 (d, 1H), 7.3 (d, 1H), 6.5 (d, 1H), 5.7 (s, 1H); C17H14N6O3S2: APCI−MS m/z 415 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369086B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-0da14ae671cb46febffcae5a1e23110e |
| Source note | uspto-grants-2002_04 |