HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfadiazine → HCID 178517001, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfadiazine | HCID 5215 | — |
| Reactant | 8-[Ethoxymethylidene]-6H-[1,3]thiazolo[5,4-e]indol-7-one | HCID 53990807 | — |
| Product | HCID 178517001 | HCID 178517001 | 29% |
Reaction Steps
The title compound was prepared in 29% yield from 8-ethoxymethylene-6,8-dihydro-1-thia-3,6-diaza-as-indacen-7-one and 4-amino-N-pyrimidin-2-yl-benzenesulfonamide according to Procedure J: 1H NMR (DMSO-d6): δ11.18 (d, 1H), 10.94 (s, 1H), 9.28 (s, 1H), 8.52 (d, 1H) 8.08 (d, 1H), 7.99 (d, 1H), 7.84 (d, 1H), 7.6 (d, 1H), 7.13 (d, 1H), 7.06 (m, 1H), 7.01 (m, 1H),; APCI−MS m/z 449 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369086B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-5b954255c9b241d5957e6a6ab4e8b242 |
| Source note | uspto-grants-2002_04 |