Methanol, 1,1-diethoxy-, 1-acetate → HCID 54066410, compound

HRID 840947Notes

Reaction equation

HRID 840947 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]1[CH:7]=[C:8]2[CH2:14][C:13](=[O:15])[NH:12][C:9]2=[N:10][CH:11]=1.[C:16]([O:19][CH:20](OCC)OCC)(=O)[CH3:17]>>[CH2:16]([O:19][CH:20]=[C:14]1[C:8]2[C:9](=[N:10][CH:11]=[C:6]([C:2]3[O:1][CH:5]=[CH:4][CH:3]=3)[CH:7]=2)[NH:12][C:13]1=[O:15])[CH3:17]

Participants

3

Reactant 2

HCID 84166Methanol, 1,1-diethoxy-, 1-acetateHCID 155040685-(Furan-2-yl)-7-aza-oxindole

Product 1

HCID 54066410HCID 54066410, compound

Procedure

This compound was synthesized from 5-(2-furyl)-1,3-dihydro-2H-pyrrolo[2,3-b]pyridin-2-one and diethoxymethyl acetate according to Procedure A. 1H NMR 400 MHz (DMSO-d6): δ10.96 (s, 1H); 8.36 (s, 1H); 7.87-7.84 (m, 2H); 7.72 (s, 1H); 6.87 (d, 1H); 6.56 (m, 1H); 4.42 (m, 2H); 1.36 (m, 3H).

Sources & evidence

ORD record
ord-317e67ec6cee4045ac4adc41dec15cbf
Source dataset
uspto-grants-2002_04
Patent number
US06369086B1

Reaction notes

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