Methanol, 1,1-diethoxy-, 1-acetate → HCID 53720546, compound

HRID 840949Notes

Reaction equation

HRID 840949 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]2[CH2:10][C:9](=[O:11])[NH:8][C:5]2=[N:6][CH:7]=1.[C:12]([O:15][CH:16](OCC)OCC)(=O)[CH3:13]>>[Br:1][C:2]1[CH:3]=[C:4]2[C:10](=[CH:16][O:15][CH2:12][CH3:13])[C:9](=[O:11])[NH:8][C:5]2=[N:6][CH:7]=1

Participants

3

Reactant 2

HCID 84166Methanol, 1,1-diethoxy-, 1-acetateHCID 155040625-bromo-1H,2H,3H-pyrrolo(2,3-b)pyridin-2-one

Product 1

HCID 53720546HCID 53720546, compound

Procedure

This compound was synthesized from 5-bromo-1H-pyrrolo[2,3-b]pyridin-2-one and and diethoxymethyl acetate according to Procedure A. 1H NMR 400 MHz (DMSO-d6): δ11.02 (s, 1H); 8.07 (s, 1H); 7.88 (s, 1H); 7.71 (s, 1H); 4.40 (m, 2H); 1.34 (m, 3H).

Sources & evidence

ORD record
ord-1b0dc67077424d9ab4ecb7e23ed0e297
Source dataset
uspto-grants-2002_04
Patent number
US06369086B1

Reaction notes

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