HCID 22620494, compound → HCID 22620520, compound
Reaction equation
CC(C)(CCC1C=CC=CC=1)CC(O)=O.[CH3:16][O:17][C:18](=[O:34])[CH:19]([C:23]([CH3:33])([CH3:32])[CH2:24][CH2:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1)[C:20]([O-])=O.CC1(C)CCC2C=CC=CC=2C(=O)C1C(OC)=O>>[CH3:32][C:23]1([CH3:33])[C:19]([C:18]([O:17][CH3:16])=[O:34])=[CH:20][C:27]2[CH:28]=[CH:29][CH:30]=[CH:31][C:26]=2[CH2:25][CH2:24]1Participants
4
Procedure
Methyl 7,7-dimethyl-6,7-dihydro-5H-benzocycloheptene-8-carboxylate was synthesized by the same process as in Reference Example 1, (b) and (c) except for using 7,7-dimethyl-6-methoxycarbonyl-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one.
Sources & evidence
- ORD record
- ord-8eab9f0d8fc040f69c2f8bcded2fb740
- Source dataset
- uspto-grants-2002_04
- Patent number
- US06369110B1
Reaction notes
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