HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → N-Octadecanoylacrylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Acrylamide | HCID 6579 | — |
| Reactant | Stearoyl chloride | HCID 8212 | — |
| Reactant | N-Hexadecylacrylamide | HCID 88828 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | N-Octadecanoylacrylamide | HCID 22620855 | — |
Reaction Steps
In a 250 ml capacity conical flask 15.1 g stearoyl chloride (0.05 M), 3.5 g acrylamide (0.05 M) and 50 ml acetone were placed to obtain a clear solution. The solution was stirred with a magnetic needle at room temperature. 6.5. g anhydrous aluminium chloride (0.05 M) was added and the reaction mixture was stirred at room temperature. After 5 to 10 minutes of stirring vigorous evolution of hydrogen chloride took place which ceased after about 5 minutes. The product was isolated following the procedure described for synthesis of N-cetylacrylamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06369249B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-d78d7bea283948b5bd38b872279b005b |
| Source note | uspto-grants-2002_04 |