Ammonium Chloride → HCID 178439813, compound

HRID 841887Notes

Reaction equation

HRID 841887 reaction equation
[CH2:1]([CH:4]1[NH:10][C:9](=S)[CH2:8][CH2:7][S:6][CH2:5]1)[CH2:2][CH3:3].F[B-](F)(F)F.C[O+](C)C.[Cl-:21].[NH4+:22]>>[ClH:21].[NH:22]=[C:9]1[CH2:8][CH2:7][S:6][CH2:5][CH:4]([CH2:1][CH2:2][CH3:3])[NH:10]1

Participants

4

Reactant 3

HCID 25517Ammonium ChlorideHCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 22617730HCID 22617730, compound

Product 1

HCID 178439813HCID 178439813, compound

Procedure

Employing the procedure described in Example 2, step D, tetrahydro-3-propyl-(2H)-1,4-thiazepin-5-thione was reacted with Meerwein's salt and ammonium chloride to yield hexahydro-5-imino-3-propyl-1,4-thiazepine, hydrochloride.

Sources & evidence

ORD record
ord-c1436535f9a04df286f7f8ffcfe6c253
Source dataset
uspto-grants-2002_04
Patent number
US06372733B1

Reaction notes

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