3,4-Dichlorophenyl isocyanate → HCID 73986449, compound

HRID 841901Notes

Reaction equation

HRID 841901 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N:9]=[C:10]=[O:11])[CH:5]=[CH:6][C:7]=1[Cl:8].[NH2:12][C:13]1[CH:14]=[C:15]2[C:19](=[CH:20][CH:21]=1)[N:18]([CH2:22][C:23]1[CH:28]=[CH:27][C:26]([Cl:29])=[C:25]([Cl:30])[CH:24]=1)[CH:17]=[C:16]2[CH:31]=[C:32]1[S:36][C:35](=[O:37])[NH:34][C:33]1=[O:38]>>[Cl:1][C:2]1[CH:3]=[C:4]([NH:9][C:10](=[O:11])[NH:12][C:13]2[CH:14]=[C:15]3[C:19](=[CH:20][CH:21]=2)[N:18]([CH2:22][C:23]2[CH:28]=[CH:27][C:26]([Cl:29])=[C:25]([Cl:30])[CH:24]=2)[CH:17]=[C:16]3[CH:31]=[C:32]2[S:36][C:35](=[O:37])[NH:34][C:33]2=[O:38])[CH:5]=[CH:6][C:7]=1[Cl:8]

Participants

3

Reactant 2

HCID 76073,4-Dichlorophenyl isocyanateHCID 73986453HCID 73986453, compound

Product 1

HCID 73986449HCID 73986449, compound

Procedure

The title compound was prepared by General Procedure 7 with 3,4-dichlorophenyl isocyanate and the amino compound from Example 47 as reactants. Nmr and ms data were consistent; ms m/e 607 (M+1). HPLC (System 1): purity greater than 80%.

Sources & evidence

ORD record
ord-d92c82ee046f4dc2aa672a9d13420fc8
Source dataset
uspto-grants-2002_04
Patent number
US06372742B1

Reaction notes

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