HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridinecarboxaldehyde → HCID 57151801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| Reactant | HCID 57243395 | HCID 57243395 | — |
| Product | HCID 57151801 | HCID 57151801 | — |
Reaction Steps
The title compound was prepared by a similar method to Preparation 35 from (3R,5S)-5-(phenoxymethyl)pyrrolidine-3-ol [see Preparation 37] and 4-pyridinecarboxaldehyde. The crude product was purified by column chromatography on silica gel eluting with a solvent system of 95:5, by volume, chloroform:methanol to afford (3R,5S)-5-(phenoxymethyl)-1-(4-pyridinylmethyl)pyrrolidine-3-ol as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06372736B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-88666ee941724898a7a0f17e3d93571a |
| Source note | uspto-grants-2002_04 |