HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 15490948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 4-(2-Bromoethoxy)Benzaldehyde | HCID 262706 | — |
| Reactant | 2-benzyl-4-methyl-1,6-dihydro-6pyrimidone | HCID 135447970 | — |
| Product | HCID 15490948 | HCID 15490948 | 20.6% |
Reaction Steps
The title compound (2.0 g, 20.6%) was prepared from 2-benzyl-4-methyl-1,6-dihydro-6-pyrimidone (5.6 g, 28.0 mmol), 4-[2-bromoethoxy]benzaldehyde (17.05 g, 30.1 mmol) in the presence of 95% NaH (873 mg, 35.0 mmol) as base by a similar procedure to that described in preparation 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06372750B2 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-918102747c044b7381c6620ab546026f |
| Source note | uspto-grants-2002_04 |