3-Cyclopentyloxy-4-methoxybenzaldehyde → HCID 10225770, compound

Participants

Reaction Steps

By employing a procedure similar to that in Example 33 and using 2-(3-chlorophenyl)-7-aminobenzoxazole (1.00 g, 0.0041 mol), 3-cyclopentyloxy-4-methoxybenzaldehyde (1.08 g, 0.0049 mol), sodium cyanoborohydride (0.41 g, 0.0065 mol) and 35 ml of methanol, a white, crystalline solid was isolated. This crude product (1.4 g) was recrystallized from 200 ml of methanol to yield the title compound (1.1 g), mp 133-134° C.

Provenance & Evidence